Technology Process of C40H39BrO5S
There total 4 articles about C40H39BrO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C12H15BrO5S;
With
sodium hydride;
In
1,4-dioxane; mineral oil;
at 20 ℃;
for 0.5h;
Inert atmosphere;
benzyl bromide;
With
tetra-(n-butyl)ammonium iodide;
In
1,4-dioxane; mineral oil;
at 60 ℃;
Inert atmosphere;
DOI:10.1016/j.carres.2014.05.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate / ethyl acetate; water / 2 h / 20 °C
2.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
2.2: pH 7 / Inert atmosphere
3.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 20 °C / Inert atmosphere
3.2: 60 °C / Inert atmosphere
With
sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; sodium carbonate;
In
1,4-dioxane; methanol; water; ethyl acetate; mineral oil;
DOI:10.1016/j.carres.2014.05.010
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
1.2: pH 7 / Inert atmosphere
2.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 20 °C / Inert atmosphere
2.2: 60 °C / Inert atmosphere
With
sodium methylate; sodium hydride;
In
1,4-dioxane; methanol; mineral oil;
DOI:10.1016/j.carres.2014.05.010
