N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

Base Information

Chemical Name:N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine
CAS No.:119772-08-6
Molecular Formula:C₃₁H₂₇N₅O₇S
Molecular Weight:613.651
Hs Code.:

N<sup>6</sup>,N<sup>6</sup>-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

Synonyms:N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

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Chemical Property of N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

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Technology Process of N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

There total 4 articles about N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 119753-67-2
N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenethio)-β-D-xylofuranosyl>adenine

: 119772-08-6
N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(01)90111-5

Reference yield:

: 2627-64-7
9-(2,3-anhydro-β-D-ribofuranosyl)adenine

: 119772-08-6
N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium methoxide / 1.) MeOH, 20 deg C, 2.) reflux

2: 1.) chlorotrimethylsilane, pyridine / 1.) 20 deg C, 2 h, 2.) 3 h

3: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With pyridine; chloro-trimethyl-silane; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)90111-5

Reference yield:

: 106-45-6
para-thiocresol

: 119772-08-6
N⁶,N⁶-dibenzoyl-9-<3'-deoxy-3'-(p-toluenesulfonyl)-β-D-xylofuranosyl>adenine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium methoxide / 1.) MeOH, 20 deg C, 2.) reflux

2: 1.) chlorotrimethylsilane, pyridine / 1.) 20 deg C, 2 h, 2.) 3 h

3: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With pyridine; chloro-trimethyl-silane; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)90111-5