C₃₆H₃₆O₉

Base Information

• Chemical Name: C₃₆H₃₆O₉
• CAS No.: 1190113-80-4
• Molecular Formula: C₃₆H₃₆O₉
• Molecular Weight: 612.676
• Mol file: 1190113-80-4.mol

Synonyms:C₃₆H₃₆O₉

Chemical Property of C₃₆H₃₆O₉

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₆H₃₆O₉

There total 2 articles about C₃₆H₃₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

Ethyl 4-hydroxybenzoate (120-47-8) + 1,3,5-Tris(bromomethyl)benzene (18226-42-1) → C36H36O9 (1190113-80-4)

Guidance literature:

With potassium carbonate; In acetone; for 7h; Reflux;

Reference yield: 50.0%

4-prop-2-ynyloxybenzoic acid ethyl ester (175203-55-1) → Ethyl 4-hydroxybenzoate (120-47-8) + C36H36O9 (1190113-92-8) + C36H36O9 (1190113-80-4)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene][3-phenyl-1H-indenylidene] ruthenium (II) dichloride; In toluene; at 80 ℃; for 112h; Inert atmosphere;

Reference yield:

C36H36O9 (1190113-80-4) → 4,4',4''-((benzene-1,3,5-triyltris(methylene))tris(oxy))tribenzoic acid (1342818-03-4)

Guidance literature:

With water; sodium hydroxide; In acetone; at 80 ℃; for 24h;

DOI:10.1016/j.ica.2019.05.005

upstream raw materials:

Ethyl 4-hydroxybenzoate

1,3,5-Tris(bromomethyl)benzene

4-prop-2-ynyloxybenzoic acid ethyl ester

Downstream raw materials:

4,4',4''-((benzene-1,3,5-triyltris(methylene))tris(oxy))tribenzoic acid