N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

Base Information

Chemical Name:N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride
CAS No.:1404223-08-0
Molecular Formula:C₁₈H₂₅Cl₂N₅*ClH
Molecular Weight:418.797
Hs Code.:

Synonyms:N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

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Chemical Property of N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

Chemical Property:

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Technology Process of N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

There total 5 articles about N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 110-89-4
piperidine

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

: 1404223-08-0
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

Guidance literature:: With mercury dichloride; In acetonitrile; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jm200503s

Reference yield:

: 6590-94-9
3,4-dichlorophenyl isothiocyanate

: 1404223-08-0
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: mercury dichloride / acetonitrile / 0.08 h / 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In dichloromethane; acetonitrile;
DOI:10.1021/jm200503s

Reference yield:

: 766449-90-5
1-isopropyl-4,5-dihydro-1H-imidazol-2-ylamine

: 1404223-08-0
N-(3,4-dichlorophenyl)-N'-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)piperidine-1-carboxamidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: mercury dichloride / acetonitrile / 0.08 h / 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In dichloromethane; acetonitrile;
DOI:10.1021/jm200503s