N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

Base Information

Chemical Name:N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester
CAS No.:1365570-70-2
Molecular Formula:C₂₁H₃₀BrNO₅
Molecular Weight:456.377
Hs Code.:

Synonyms:N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

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Chemical Property of N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

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Technology Process of N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

There total 2 articles about N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1350562-63-8
C₁₈H₂₈BrNO₅

: 106-96-7
propargyl bromide

: 1365570-70-2
N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

Guidance literature:: C₁₈H₂₈BrNO₅; With potassium carbonate; In acetonitrile; for 0.5h; Inert atmosphere;

propargyl bromide; In acetonitrile; at 40 ℃; for 8h; Inert atmosphere;
DOI:10.1007/s11164-011-0429-1

Reference yield:

: 153179-99-8
C₁₄H₂₀Br₂O₃

: 1365570-70-2
N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 20 °C

2.1: potassium carbonate / acetonitrile / 0.5 h / Inert atmosphere

2.2: 8 h / 40 °C / Inert atmosphere

With potassium carbonate; potassium hydroxide; In ethanol; acetonitrile;
DOI:10.1007/s11164-011-0429-1

Reference yield: 44.0%

: 1365570-70-2
N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] 4-aminobutyric acid propargyl ester

: 24345-72-0
1,4-diazidobutane

: (1-(4-azidobutyl)-1H-1,2,3-triazol-4-yl)methyl 4-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)butanoate

Guidance literature:: With copper(II) acetate monohydrate; copper; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1080/00397911.2014.914220