Technology Process of 1,3,5-tribromo-2,4,6-tri(hydroxyiminomethyl)benzene
There total 5 articles about 1,3,5-tribromo-2,4,6-tri(hydroxyiminomethyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium acetate;
In
ethanol;
at 60 ℃;
for 2h;
DOI:10.5560/ZNB.2012-0092
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride; bromine / 0 - 20 °C
2.1: bromine / ethylene dibromide / 20 h / Reflux
3.1: potassium acetate / N,N-dimethyl-formamide / 20 h / 80 °C
3.2: 24 h / 90 °C
4.1: pyridinium chlorochromate / dichloromethane / 48 h / 25 °C / Molecular sieve
5.1: sodium acetate; hydroxylamine hydrochloride / ethanol / 2 h / 60 °C
With
aluminum (III) chloride; hydroxylamine hydrochloride; bromine; potassium acetate; sodium acetate; pyridinium chlorochromate;
In
ethanol; dichloromethane; ethylene dibromide; N,N-dimethyl-formamide;
DOI:10.1039/c9cc09617e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine / ethylene dibromide / 20 h / Reflux
2.1: potassium acetate / N,N-dimethyl-formamide / 20 h / 80 °C
2.2: 24 h / 90 °C
3.1: pyridinium chlorochromate / dichloromethane / 48 h / 25 °C / Molecular sieve
4.1: sodium acetate; hydroxylamine hydrochloride / ethanol / 2 h / 60 °C
With
hydroxylamine hydrochloride; bromine; potassium acetate; sodium acetate; pyridinium chlorochromate;
In
ethanol; dichloromethane; ethylene dibromide; N,N-dimethyl-formamide;
DOI:10.1039/c9cc09617e
