(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

Base Information

Chemical Name:(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)
CAS No.:1449303-30-3
Molecular Formula:C₁₇H₃₃N₂OP
Molecular Weight:312.436
Hs Code.:

Synonyms:(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

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Technology Process of (trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

There total 3 articles about (trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1449303-06-3
mesitylphosphonic acid bis(N,N-diethylamide)

: 1449303-30-3
(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201300344

Reference yield:

: 90928-94-2
bis(diethylamino)-2,4,6-trimethylphenylphosphine

: 1449303-30-3
(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

2: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; dihydrogen peroxide; sodium; In tetrahydrofuran; diethyl ether; 2: |Birch Reduction;
DOI:10.1002/ejoc.201300344

Reference yield:

: 685-83-6
bis(diethylamino)chlorophosphine

: 1449303-30-3
(trans-2,4,6-trimethylcyclohexa-1,4-dien-3-yl)phosphonic acid bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium / diethyl ether; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Schlenk technique

2: dihydrogen peroxide / diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

3: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; dihydrogen peroxide; sodium; magnesium; In tetrahydrofuran; diethyl ether; 3: |Birch Reduction;
DOI:10.1002/ejoc.201300344