(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

Base Information

Chemical Name:(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate
CAS No.:125458-52-8
Molecular Formula:C₃₃H₄₄O₃S
Molecular Weight:520.777
Hs Code.:

Synonyms:(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

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Chemical Property of (6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

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Technology Process of (6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

There total 7 articles about (6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 125458-50-6
Benzoic acid (3E,7E,11E)-1-isobutyryl-3,7,11-trimethyl-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

: 125458-52-8
(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h; Ambient temperature;

Reference yield:

: 31236-13-2,60441-27-2,69538-05-2,69538-06-3,69659-77-4,69659-78-5,74986-29-1
10,11-oxido-E,E-farnesyl phenyl sulfide

: 125458-52-8
(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / aluminium isopropoxide / toluene / 12 h / Heating

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

With sodium tetrahydroborate; 2,4-Dinitrophenol; aluminum isopropoxide; In methanol; toluene;

Reference yield:

: 91496-44-5
3-methyl-2-oxybutyl benzoate

: 125458-52-8
(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / p-TsOH / methanol / 13 h / 50 °C

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

With sodium tetrahydroborate; 2,4-Dinitrophenol; toluene-4-sulfonic acid; In methanol; toluene;