((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Base Information

Chemical Name:((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol
CAS No.:225233-47-6
Molecular Formula:C₁₇H₂₄O₇
Molecular Weight:340.373
Hs Code.:

Synonyms:((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Suppliers and Price of ((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of ((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of ((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

There total 5 articles about ((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 154799-94-7
3-O-(4-Methoxybenzyl)-1,2-O-isopropylidene-4-formylerythrofuranose

: 225233-47-6
((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 46h;
DOI:10.1271/bbb.63.736

Reference yield:

: 69940-02-9,142226-15-1,115693-78-2
3-O-(4-Methoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 225233-47-6
((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / AcOH / H₂O / 21 h / 20 °C

2: NaIO₄ / H₂O / 1.5 h / 20 °C

3: NaOH / H₂O; tetrahydrofuran / 46 h / 20 °C

With sodium hydroxide; sodium periodate; acetic acid; In tetrahydrofuran; water; 1: Hydrolysis / 2: Oxidation / 3: Condensation;
DOI:10.1271/bbb.63.736

Reference yield:

: 69940-04-1,142226-16-2,109536-51-8
(R)-1-[(3aR,5R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethane-1,2-diol

: 225233-47-6
((3aR,6S,6aR)-6-((4-methoxybenzyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole-5,5-diyl)dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: NaIO₄ / H₂O / 1.5 h / 20 °C

2: NaOH / H₂O; tetrahydrofuran / 46 h / 20 °C

With sodium hydroxide; sodium periodate; In tetrahydrofuran; water; 1: Oxidation / 2: Condensation;
DOI:10.1271/bbb.63.736