N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

Base Information

Chemical Name:N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine
CAS No.:132884-68-5
Molecular Formula:C₄₅H₅₂N₂O₁₁
Molecular Weight:796.915
Hs Code.:

Synonyms:N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

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Chemical Property of N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

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Technology Process of N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

There total 2 articles about N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 30925-18-9
2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

: 77611-19-9
2-O-Acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

: 132884-68-5
N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1021/jo00011a050

Reference yield:

: 133004-71-4
(3aS,5R,6R,7S,7aR)-6,7-bis(benzyloxy)-5-<(benzyloxy)-methyl>-2-methyl-5H-pyrano<2,3-d>oxazole

: 132884-68-5
N-<1-benzyl N-(tert-butyloxycarbonyl)-4-L-aspartyl>-2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / H₂O, 1N HCl / tetrahydrofuran / 0.5 h / Ambient temperature

2: 80 percent / DMAP, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride (EDCI) / dimethylformamide / 18 h / Ambient temperature

With hydrogenchloride; dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00011a050