C₃₇H₅₂N₈O₁₀

Base Information

Chemical Name:C₃₇H₅₂N₈O₁₀
CAS No.:958945-43-2
Molecular Formula:C₃₇H₅₂N₈O₁₀
Molecular Weight:768.867
Hs Code.:

C<sub>37</sub>H<sub>52</sub>N<sub>8</sub>O<sub>10</sub>

Synonyms:C₃₇H₅₂N₈O₁₀

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Chemical Property of C₃₇H₅₂N₈O₁₀

Chemical Property:

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Technology Process of C₃₇H₅₂N₈O₁₀

There total 11 articles about C₃₇H₅₂N₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1262483-42-0
C₃₃H₄₅N₅O₇

: 162463-99-2
(S)-2-azido-3-hydroxypropionic acid methyl ester

: 958945-43-2
C₃₇H₅₂N₈O₁₀

Guidance literature:: With copper; copper(II) sulfate; In tetrahydrofuran; water; at 25 ℃; Inert atmosphere;
DOI:10.1021/ja1071916

Reference yield:

: 810681-06-2
3-bromo-5-iodobenzoyl chloride

: 958945-43-2
C₃₇H₅₂N₈O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 11 h / 25 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 70 °C / Inert atmosphere

4: water; sodium hydroxide / methanol / 18 h / 25 °C / Inert atmosphere

5: copper; copper(II) sulfate / tetrahydrofuran; water / 25 °C / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

7: copper; copper(II) sulfate / tetrahydrofuran; water / 25 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; water; copper; copper(II) sulfate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja1071916

Reference yield:

: 1192373-19-5
C₁₆H₂₀BrIN₂O₃

: 958945-43-2
C₃₇H₅₂N₈O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 70 °C / Inert atmosphere

3: water; sodium hydroxide / methanol / 18 h / 25 °C / Inert atmosphere

4: copper; copper(II) sulfate / tetrahydrofuran; water / 25 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

6: copper; copper(II) sulfate / tetrahydrofuran; water / 25 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; water; copper; copper(II) sulfate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1021/ja1071916