N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Base Information

Chemical Name:N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide
CAS No.:129966-18-3
Molecular Formula:C₂₃H₃₁NO₃S
Molecular Weight:401.57
Hs Code.:

N-ethyl-N-<<trans-(2-phenylcyclohexyl)oxy>carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Synonyms:N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Chemical Property:

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Technology Process of N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

There total 4 articles about N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 368-39-8
triethyloxonium fluoroborate

: 107575-45-1,130060-13-8,130060-14-9
N-<carbonyl>-cis-bicyclo<3.3.0>-3-oct-endo-2-enesulfinamide

: 129966-18-3
N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -10 ℃; for 0.5h;
DOI:10.1021/ja00177a029

Reference yield:

: 129966-10-5
(S)-trans-2-phenylcyclohexyl carbamate

: 129966-18-3
N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine, SOCl₂ / benzene / 0.25 h

2: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

3: Huenig's base / CH₂Cl₂ / 0.5 h / -10 °C

With pyridine; thionyl chloride; tin(IV) chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; benzene;
DOI:10.1021/ja00177a029

Reference yield:

: 107575-41-7,130060-02-5
(S)-trans-2-phenylcyclohexyl N-sulfinylcarbamate

: 129966-18-3
N-ethyl-N-<carbonyl>bicyclo<3.3.0>-3-oct-2-enesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

2: Huenig's base / CH₂Cl₂ / 0.5 h / -10 °C

With tin(IV) chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ja00177a029