Technology Process of C21H23BrO3
There total 7 articles about C21H23BrO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 48h;
Reflux;
DOI:10.1021/ol302011b
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / acetone / 6 h / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Reflux
3: water; potassium carbonate / methanol; ethyl acetate
4: N-Bromosuccinimide; silica gel / dichloromethane / 20 °C
5: potassium carbonate / acetone / 48 h / Reflux
With
N-Bromosuccinimide; water; silica gel; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; ethyl acetate; acetone;
2: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1021/ol302011b
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetone / Reflux
2: potassium carbonate / acetone / 6 h / Reflux
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Reflux
4: water; potassium carbonate / methanol; ethyl acetate
5: N-Bromosuccinimide; silica gel / dichloromethane / 20 °C
6: potassium carbonate / acetone / 48 h / Reflux
With
N-Bromosuccinimide; water; silica gel; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; ethyl acetate; acetone;
3: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1021/ol302011b
