carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

Base Information

Chemical Name:carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester
CAS No.:773056-53-4
Molecular Formula:C₁₃H₁₆N₂O₄S
Molecular Weight:296.347
Hs Code.:

Synonyms:carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

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Chemical Property of carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

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Technology Process of carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

There total 5 articles about carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2,2,2-Trichloro-acetyl)-carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

: 773056-53-4
carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 2h;
DOI:10.1021/jo048990k

Reference yield:

: 773056-51-2
N-allyl-N-(2-hydroxymethylallyl)-4-methylbenzenesulfonamide

: 773056-53-4
carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / Grubbs' catalyst / CH₂Cl₂ / 34 h / 40 °C

2: CH₂Cl₂ / 3 h / 20 °C

3: K₂CO₃ / methanol / 2 h / 25 °C

With potassium carbonate; Grubbs catalyst first generation; In methanol; dichloromethane;
DOI:10.1021/jo048990k

Reference yield:

: 773056-50-1
2-[[allyl(toluene-4-sulfonyl)amino]methyl]acrylic acid ethyl ester

: 773056-53-4
carbamic acid 1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / DIBAL-H / diethyl ether / -78 - 25 °C

2: 63 percent / Grubbs' catalyst / CH₂Cl₂ / 34 h / 40 °C

3: CH₂Cl₂ / 3 h / 20 °C

4: K₂CO₃ / methanol / 2 h / 25 °C

With diisobutylaluminium hydride; potassium carbonate; Grubbs catalyst first generation; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo048990k