Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Base Information

Chemical Name:Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester
CAS No.:183429-92-7
Molecular Formula:C₉₅H₁₃₀NO₂₁P₃
Molecular Weight:1714.99
Hs Code.:

Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Synonyms:Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

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Chemical Property of Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

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Technology Process of Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

There total 1 articles about Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 183429-89-2
Hexadecanoic acid (R)-2-[((1S,2R,3R,4S,5S,6R)-2,6-bis-benzyloxymethoxy-3,4,5-trihydroxy-cyclohexyloxy)-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

: 183429-92-7
Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 24 deg C, 1 h, 2.) CH₂Cl₂, -40 deg C, 1 h;
DOI:10.1021/jo961226g

Reference yield: 93.0%

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: 183429-92-7
Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

: 2,6-O-bis(benzyloxymethyl)-3-O-(benzyloxy)-4,5-O-bis(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl diisopropylethylammonium phosphate

Guidance literature:: In acetonitrile; at 60 ℃; for 12h;
DOI:10.1021/jo961226g

Reference yield: 72.0%

: 183429-92-7
Hexadecanoic acid (R)-2-[[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

: 4,5-di-O-phosphoryl-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 3-aminopropyl phosphate sodium salt

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In water; tert-butyl alcohol; for 21h; under 2637.5 Torr;
DOI:10.1021/jo961226g