benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

Base Information

Chemical Name:benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside
CAS No.:1192256-38-4
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

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Technology Process of benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

There total 1 articles about benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 591-80-0
pent-4-enoic acid

: 1192256-21-5
benzyl 4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

: 1192256-38-4
benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; for 4h;
DOI:10.1016/j.tet.2009.07.088

Reference yield: 12.0%

: 74-85-1
ethene

: 1192256-38-4
benzyl 4-O-(2-butynyl)-6-O-(pent-4-enoyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

: C₂₂H₂₆O₅

: C₂₂H₂₆O₅

: 1192256-59-9
C₂₄H₃₀O₅

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Reflux;
DOI:10.1016/j.tet.2009.07.088