C₄₄H₆₃ClN₄O₃

Base Information

Chemical Name:C₄₄H₆₃ClN₄O₃
CAS No.:1449797-63-0
Molecular Formula:C₄₄H₆₃ClN₄O₃
Molecular Weight:731.462
Hs Code.:

C<sub>44</sub>H<sub>63</sub>ClN<sub>4</sub>O<sub>3</sub>

Synonyms:C₄₄H₆₃ClN₄O₃

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Chemical Property of C₄₄H₆₃ClN₄O₃

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Technology Process of C₄₄H₆₃ClN₄O₃

There total 15 articles about C₄₄H₆₃ClN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 68055-38-9
4-Chloro-N-(2-dimethylamino-ethyl)-thiobenzamide

: 1449796-78-4
C₃₃H₅₂N₂O₄

: 1449797-63-0
C₄₄H₆₃ClN₄O₃

Guidance literature:: With silver benzoate; acetic acid; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 473-98-3
betulin

: 1449797-63-0
C₄₄H₆₃ClN₄O₃

Guidance literature:: Multi-step reaction with 12 steps

1: toluene / 3 h / 100 °C

2: acetic anhydride; hydrogen bromide; acetic acid / toluene / 1.5 h / 105 °C

3: acetic anhydride; acetic acid; sodium acetate; sodium dichromate / toluene / 60 °C

4: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

5: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C

6: triethylamine / 20 °C

7: toluene-4-sulfonic acid / 20 °C

8: sodium tetrahydroborate; methanol / 1 h / 20 °C / Cooling with ice

9: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

10: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

11: hydrazine hydrate / dichloromethane / 0.5 h / 0 °C

12: acetic acid; silver benzoate / dichloromethane / 48 h / 20 °C

With methanol; sodium tetrahydroborate; sodium dichromate; oxalyl dichloride; hydrogen bromide; sodium acetate; silver benzoate; acetic anhydride; silica gel; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; potassium hydroxide; sodium nitrite; In ethanol; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 1721-69-3
betulin diacetate

: 1449797-63-0
C₄₄H₆₃ClN₄O₃

Guidance literature:: Multi-step reaction with 11 steps

1: acetic anhydride; hydrogen bromide; acetic acid / toluene / 1.5 h / 105 °C

2: acetic anhydride; acetic acid; sodium acetate; sodium dichromate / toluene / 60 °C

3: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

4: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C

5: triethylamine / 20 °C

6: toluene-4-sulfonic acid / 20 °C

7: sodium tetrahydroborate; methanol / 1 h / 20 °C / Cooling with ice

8: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

9: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

10: hydrazine hydrate / dichloromethane / 0.5 h / 0 °C

11: acetic acid; silver benzoate / dichloromethane / 48 h / 20 °C

With methanol; sodium tetrahydroborate; sodium dichromate; oxalyl dichloride; hydrogen bromide; sodium acetate; silver benzoate; acetic anhydride; silica gel; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; potassium hydroxide; sodium nitrite; In ethanol; dichloromethane; dimethyl sulfoxide; toluene;