(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

Base Information

Chemical Name:(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate
CAS No.:1036233-14-3
Molecular Formula:C₁₈H₂₆O₅S
Molecular Weight:354.467
Hs Code.:

Synonyms:(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

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Technology Process of (S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

There total 1 articles about (S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 952517-39-4
C₁₁H₂₀O₃

: 98-59-9
p-toluenesulfonyl chloride

: 1036233-14-3
(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at -2 - 6 ℃; for 4h;

Reference yield: 73.8%

: 300355-14-0
(3-chloro-4-methylsulfanylphenyl)acetic acid ethyl ester

: 1036233-14-3
(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate

: 952517-42-9
2-(3-chloro-4-(methylsulfonyl)phenyl)-3-(8,8-dimethyl-6,10-dioxaspiro[4.5]-decan-2(R)-yl)propanoic acid

Guidance literature:: (3-chloro-4-methylsulfanylphenyl)acetic acid ethyl ester; With potassium tert-butylate; In tetrahydrofuran; at -15 ℃; for 2h;

(S)-(8,8-dimethyl-6,10-dioxaspiro[4.5]decan-2-yl)methyl 4-methylbenzenesulfonate; In tetrahydrofuran; at 0 - 40 ℃;

With sodium hydroxide; sodium tungstate; dihydrogen peroxide; sodium hydrogencarbonate; more than 3 stages;