diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

Base Information

Chemical Name:diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate
CAS No.:1293393-69-7
Molecular Formula:C₃₁H₄₁N₂O₇P
Molecular Weight:584.649
Hs Code.:

Synonyms:diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

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Chemical Property of diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

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Technology Process of diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

There total 1 articles about diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53753-37-0
diethyl (nitromethyl)phosphonate

: 51091-84-0
(S)-naproxenoyl chloride

: 271600-36-3
N-[phenyl(toluene-4-sulfonyl)methyl]tert-butoxycarboxyamide

: diethyl {(1R,2R)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

: 1293393-69-7
diethyl {(1S,2S)-(2-tert-butoxycarbonylamino)-1-[(S)-2-(6-methoxynaphthalen-2-yl)propionylamino]-2-phenyl-ethyl}phosphonate

Guidance literature:: diethyl (nitromethyl)phosphonate; N-[phenyl(toluene-4-sulfonyl)methyl]tert-butoxycarboxyamide; With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((S)-(6-methoxyquinolin-4-yl)((2S,4S,8R)-8-vinylquinuclidin-2-yl)methyl)thiourea; potassium carbonate; In toluene; at 20 ℃; for 72h;

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; at -30 - 0 ℃;

(S)-naproxenoyl chloride; With pyridine; In chloroform-d1; at 20 ℃; for 1h; optical yield given as %de;
DOI:10.1016/j.tet.2010.10.072