{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester
CAS No.:98625-46-8
Molecular Formula:C₄₂H₅₆N₈O₉S
Molecular Weight:849.021
Hs Code.:

{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Synonyms:{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

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Chemical Property of {1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

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Technology Process of {1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

There total 10 articles about {1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98625-45-7
2-(2-{2-[2-(2-tert-Butoxycarbonylamino-3-tritylsulfanyl-propionylamino)-acetylamino]-3-carbamoyl-propionylamino}-4-methyl-pentanoylamino)-3-hydroxy-propionic acid methyl ester

: 98625-46-8
{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: With hydrazine hydrate; In methanol; N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1007/BF00574212

Reference yield:

: 13139-15-6,53296-34-7
Boc-DL-Leu-OH

: 98625-46-8
{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1) C₂H₅OCOCl

2: HCl / ethyl acetate

4: 98 percent / HCl / methanol

5: 59.8 percent / (C₂H₅)3N / dimethylformamide / 40 h / Ambient temperature

6: 82 percent / N₂H₄*H₂O / methanol; dimethylformamide / 24 h / Ambient temperature

With hydrogenchloride; chloroformic acid ethyl ester; hydrazine hydrate; triethylamine; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1007/BF00574212

Reference yield:

: 1123171-13-0
N-(tert-butoxycarbonyl)-S-triphenylmethylcysteine

: 98625-46-8
{1-[({2-Carbamoyl-1-[1-(1-hydrazinocarbonyl-2-hydroxy-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-ethylcarbamoyl}-methyl)-carbamoyl]-2-tritylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: (C₂H₅)3N / CH₂Cl₂ / 0.33 h / -20 °C

3: 1,3-dicyclohexylcarbodiimide / dioxane / 7 °C

4: 59.8 percent / (C₂H₅)3N / dimethylformamide / 40 h / Ambient temperature

5: 82 percent / N₂H₄*H₂O / methanol; dimethylformamide / 24 h / Ambient temperature

With hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/BF00574212