7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

Base Information

Chemical Name:7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine
CAS No.:1356922-27-4
Molecular Formula:C₃₈H₂₃N₃S
Molecular Weight:553.687
Hs Code.:

Synonyms:7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

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Chemical Property of 7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

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Technology Process of 7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

There total 5 articles about 7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

aqueous potassium carbonate: aqueous potassium carbonate

: 1307859-67-1
((3-(dibenzo[b,d]thiophen-4-yl)phenyl)boronic acid)

: 1356922-24-1
7-bromo-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

: 1356922-27-4
7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

Guidance literature:: With sodium bicarbonate; tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In methanol; ethanol; chloroform; water; toluene;

Reference yield: 66.0%

: 1307859-67-1
((3-(dibenzo[b,d]thiophen-4-yl)phenyl)boronic acid)

: 1356922-24-1
7-bromo-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

: 1356922-27-4
7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 100 ℃; for 7h; Inert atmosphere;

Reference yield:

: 1356922-26-3
N'-benzoyl-N-(2-bromophenanthridin-6-yl)hydrazine

: 1356922-27-4
7-[3-(dibenzothiophen-4-yl)phenyl]-3-phenyl-1,2,4-triazolo[4,3-f]phenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 6 h / 120 °C / Inert atmosphere

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 7 h / 100 °C / Inert atmosphere

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; N,N-dimethyl-formamide; toluene;