butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

Base Information

Chemical Name:butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate
CAS No.:1352726-56-7
Molecular Formula:C₃₅H₃₉Cl₂N₃O₆
Molecular Weight:668.617
Hs Code.:

Synonyms:butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

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Chemical Property of butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

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Technology Process of butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

There total 3 articles about butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352729-97-5
chloro(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

: 107-92-6
butyric acid

: 1352726-56-7
butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

Reference yield:

: 100-52-7
benzaldehyde

: 1352726-56-7
butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / diethyl ether / -20 - 20 °C / Inert atmosphere

2.1: sodium hydride / 2-methyltetrahydrofuran / 1.5 h / Reflux

2.2: 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C

With pyridine; sodium hydride; caesium carbonate; In 2-methyltetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 81363-09-9
α-chlorobenzyl chloroformate

: 129722-12-9
aripiprazole

: 1352726-56-7
butyryloxy(phenyl)methyl 7-(4-(4-(2,3-dichlorophenyl)piperazin-1-yl)butoxy)-2-oxo-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / 2-methyltetrahydrofuran / 1.5 h / Reflux

1.2: 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C

With sodium hydride; caesium carbonate; In 2-methyltetrahydrofuran; N,N-dimethyl-formamide;