6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide

Base Information

• Chemical Name: 6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide
• CAS No.: 211918-63-7
• Molecular Formula: C₂₈H₃₁NOS
• Molecular Weight: 429.626
• Mol file: 211918-63-7.mol

Synonyms:6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide

Chemical Property of 6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide

There total 1 articles about 6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzenesulfenyl chloride (931-59-9) + 6,6-diphenyl-hex-5-enoic acid butylamide (211918-53-5) → 6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide (211918-63-7)

Guidance literature:

6,6-diphenyl-hex-5-enoic acid butylamide; With sodium hydride; In tetrahydrofuran; for 4h; Heating;

benzenesulfenyl chloride; In tetrahydrofuran; at -78 ℃;

DOI:10.1021/ja981244a

Reference yield:

6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide (211918-63-7) → N-butyl-6,6-diphenyl-hex-5-enimidoyl chloride

Guidance literature:

Multi-step reaction with 2 steps

1: Bu₃SnH / 5 h

2: COCl₂; DMF / benzene; toluene / 5 - 20 °C

With tri-n-butyl-tin hydride; N,N-dimethyl-formamide; In toluene; benzene;

DOI:10.1021/ja981244a

Reference yield:

6,6-diphenyl-hex-5-enoic acid butyl-phenylsulfanyl-amide (211918-63-7) → C23H26ClNO2

Guidance literature:

Multi-step reaction with 3 steps

1: Bu₃SnH / 5 h

2: Et₃N / diethyl ether / 12 h / 20 °C

3: diethyl ether; toluene / 5 - 20 °C

With tri-n-butyl-tin hydride; triethylamine; In diethyl ether; toluene;

DOI:10.1021/ja981244a

upstream raw materials:

benzenesulfenyl chloride

6,6-diphenyl-hex-5-enoic acid butylamide

Downstream raw materials:

6,6-diphenyl-hex-5-enoic acid butylamide