S-(2,6-dimethyl)phenyl α-chlorothioacetate

Base Information

Chemical Name:S-(2,6-dimethyl)phenyl α-chlorothioacetate
CAS No.:1262984-77-9
Molecular Formula:C₁₀H₁₁ClOS
Molecular Weight:214.716
Hs Code.:

Synonyms:S-(2,6-dimethyl)phenyl α-chlorothioacetate

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Chemical Property of S-(2,6-dimethyl)phenyl α-chlorothioacetate

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Technology Process of S-(2,6-dimethyl)phenyl α-chlorothioacetate

There total 1 articles about S-(2,6-dimethyl)phenyl α-chlorothioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 118-72-9
2,6-dimethylbenzene-1-thiol

: 79-04-9
chloroacetyl chloride

: 1262984-77-9
S-(2,6-dimethyl)phenyl α-chlorothioacetate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0cc02345k

Reference yield:

: 1262984-77-9
S-(2,6-dimethyl)phenyl α-chlorothioacetate

: 66-99-9
β-naphthaldehyde

: C₂₁H₁₉ClO₂S

: C₂₁H₁₉ClO₂S

Guidance literature:: S-(2,6-dimethyl)phenyl α-chlorothioacetate; β-naphthaldehyde; With magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

optical yield given as %de; diastereoselective reaction; Inert atmosphere; Acidic aq. solution;
DOI:10.1039/c0cc02345k