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(2S,4S)-Nα-Cbz-4-azidoproline benzyl ester

Base Information Edit
  • Chemical Name:(2S,4S)-Nα-Cbz-4-azidoproline benzyl ester
  • CAS No.:329191-55-1
  • Molecular Formula:C20H20N4O4
  • Molecular Weight:380.403
  • Hs Code.:
  • Mol file:329191-55-1.mol
(2S,4S)-N<sup>α</sup>-Cbz-4-azidoproline benzyl ester

Synonyms:(2S,4S)-Nα-Cbz-4-azidoproline benzyl ester

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Chemical Property of (2S,4S)-Nα-Cbz-4-azidoproline benzyl ester Edit
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Technology Process of (2S,4S)-Nα-Cbz-4-azidoproline benzyl ester

There total 6 articles about (2S,4S)-Nα-Cbz-4-azidoproline benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium azide; In N,N-dimethyl-formamide; at 65 - 70 ℃; for 8h;
DOI:10.1021/jo005626m
Guidance literature:
Multi-step reaction with 2 steps
1: 80 percent / pyridine / 48 h / 20 °C
2: 80 percent / NaN3 / dimethylformamide; H2O / 48 h / 70 °C
With sodium azide; In pyridine; water; N,N-dimethyl-formamide;
DOI:10.1002/adsc.200505058
Guidance literature:
Multi-step reaction with 3 steps
1.1: Et3N / tetrahydrofuran / 0.5 h / 0 °C
1.2: 70 percent / tetrahydrofuran / 24 h / Heating
2.1: 80 percent / pyridine / 48 h / 20 °C
3.1: 80 percent / NaN3 / dimethylformamide; H2O / 48 h / 70 °C
With sodium azide; triethylamine; In tetrahydrofuran; pyridine; water; N,N-dimethyl-formamide;
DOI:10.1002/adsc.200505058
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