N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Base Information

Chemical Name:N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene
CAS No.:124400-48-2
Molecular Formula:C₂₃H₂₂N₂O₃S
Molecular Weight:406.505
Hs Code.:

N<sup>4</sup>-Benzoyl-N<sup>1</sup>-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Synonyms:N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Suppliers and Price of N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

There total 4 articles about N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 124400-30-2
N⁴-Benzoyl-N¹-(phenylsulfonyl)-p-benzoquinone Diimine

: 35998-93-7
tri-n-butylcrotyltin

: 124400-48-2
N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; 1) -78 deg C, 12 h, 2) -20 deg C, 12 h;
DOI:10.1021/jo00291a059

Reference yield:

: 3393-96-2
p-nitrobenzanilide

: 124400-48-2
N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h / 25 °C / 2585.7 Torr

2: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating

3: 79 percent / lead tetraacetate / CHCl₃ / 12 h / 25 °C

4: 54 percent / BF₃*Et₂O / CH₂Cl₂ / 1) -78 deg C, 12 h, 2) -20 deg C, 12 h

With pyridine; lead(IV) acetate; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jo00291a059

Reference yield:

: 17625-83-1
N-(4-aminophenyl)benzamide

: 124400-48-2
N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diamino-2-<3-(3-methyl-1-propenyl)>benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating

2: 79 percent / lead tetraacetate / CHCl₃ / 12 h / 25 °C

3: 54 percent / BF₃*Et₂O / CH₂Cl₂ / 1) -78 deg C, 12 h, 2) -20 deg C, 12 h

With pyridine; lead(IV) acetate; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/jo00291a059