3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

Base Information

Chemical Name:3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester
CAS No.:107222-88-8
Molecular Formula:C₂₆H₃₁NO₉
Molecular Weight:501.533
Hs Code.:

Synonyms:3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

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Chemical Property of 3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

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Technology Process of 3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

There total 1 articles about 3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 107222-85-5,107222-86-6
2-Benzyloxycarbonylamino-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-3-hydroxy-propionic acid

: 107222-88-8
3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

: 107222-87-7
3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-L-glycero-β-L-ido-heptofuranuronsaeure-methylester

Guidance literature:: In methanol; diethyl ether; Yield given. Yields of byproduct given;

Reference yield: 86.0%

: 108-24-7
acetic anhydride

: 107222-88-8
3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

: 107222-92-4
6-Acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

Guidance literature:: With hydrogen; nickel; In methanol; for 2h;

Reference yield:

: 107222-88-8
3-O-Benzyl-6-(benzyloxycarbonylamino)-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranuronsaeure-methylester

: 95580-81-7
6-Acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / H₂ / Raney-nickel / methanol / 2 h

2: 62 percent / LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; nickel; In tetrahydrofuran; methanol;