Technology Process of C20H27N3O7
There total 6 articles about C20H27N3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1: sodium hydride / tetrahydrofuran / 10 h / 0 °C / Reflux
2: hydrazine hydrate / isopropyl alcohol / 20 °C
3: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C
4: palladium 10% on activated carbon; hydrogen / methanol; water / 20 °C
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonia / water; N,N-dimethyl-formamide / 20 °C
6: sodium methylate / methanol / 3 h / 20 °C
With
palladium 10% on activated carbon; ammonia; hydrogen; sodium methylate; benzyltri(n-butyl)ammonium chloride; sodium hydride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrazine hydrate / isopropyl alcohol / 20 °C
2: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol; water / 20 °C
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonia / water; N,N-dimethyl-formamide / 20 °C
5: sodium methylate / methanol / 3 h / 20 °C
With
palladium 10% on activated carbon; ammonia; hydrogen; sodium methylate; benzyltri(n-butyl)ammonium chloride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041