rac-isopropylmethylphenylsilane

Base Information

Chemical Name:rac-isopropylmethylphenylsilane
CAS No.:76622-52-1
Molecular Formula:C₁₀H₁₆Si
Molecular Weight:164.323
Hs Code.:

Synonyms:rac-isopropylmethylphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-isopropylmethylphenylsilane

Chemical Property:

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Technology Process of rac-isopropylmethylphenylsilane

There total 4 articles about rac-isopropylmethylphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: isopropylmethylphenyl(1-phenylethoxy)silane

: 98-85-1,13323-81-4
1-Phenylethanol

: 76622-52-1
rac-isopropylmethylphenylsilane

Guidance literature:: With diisobutylaluminium hydride; In hexane; at 20 ℃; for 20h; Schlenk technique; Reflux;
DOI:10.1021/ja503254f

Reference yield: 54.0%

: 40299-93-2
rac-isopropylmethoxymethylphenylsilane

: 76622-52-1
rac-isopropylmethylphenylsilane

Guidance literature:: With diisobutylaluminium hydride; In hexane; at 0 - 20 ℃; for 12.3333h; Inert atmosphere;
DOI:10.1002/ejoc.200900796

Reference yield:

: 3027-21-2
dimethoxy(methyl)phenylsilane

: 76622-52-1
rac-isopropylmethylphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / tetrahydrofuran / 16 h / Heating

2: LiAlH₄ / tetrahydrofuran / 10 h / Heating

With lithium aluminium tetrahydride; magnesium; In tetrahydrofuran;
DOI:10.1016/0022-328X(85)80241-2