Technology Process of C39H49N3O9
There total 5 articles about C39H49N3O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Grubbs catalyst first generation;
In
toluene;
at 65 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/jo2011957
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.05 h / 0 - 25 °C / Inert atmosphere
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 25 °C / Inert atmosphere
3: Grubbs catalyst first generation / toluene / 4 h / 65 °C / Inert atmosphere
With
Grubbs catalyst first generation; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil;
3: Ring-closure metathesis;
DOI:10.1021/jo2011957
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere
1.2: 2.03 h / 0 - 23 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.05 h / 0 - 25 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 25 °C / Inert atmosphere
4.1: Grubbs catalyst first generation / toluene / 4 h / 65 °C / Inert atmosphere
With
Grubbs catalyst first generation; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil;
4.1: Ring-closure metathesis;
DOI:10.1021/jo2011957
