3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

Base Information

Chemical Name:3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole
CAS No.:1372602-87-3
Molecular Formula:C₂₇H₂₈N₄
Molecular Weight:408.546
Hs Code.:

Synonyms:3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

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Chemical Property of 3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

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Technology Process of 3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

There total 4 articles about 3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 772-38-3
4-tert-Butylphenylacetylene

: 1372602-76-0
3-(1-azidoethyl)-9-methyl-9H-carbazole

: 1372602-87-3
3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; 4-nitro-benzoic acid; In water; tert-butyl alcohol; at 20 ℃; for 1h;
DOI:10.1021/jm300125e

Reference yield:

: 10523-06-5
1-(9-methyl-9H-carbazol-3-yl)ethanol

: 1372602-87-3
3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) chloride; trimethylsilylazide / nitromethane / 0.5 h / 60 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate; 4-nitro-benzoic acid / water; tert-butyl alcohol / 1 h / 20 °C

With indium(III) chloride; copper(ll) sulfate pentahydrate; trimethylsilylazide; sodium L-ascorbate; 4-nitro-benzoic acid; In nitromethane; water; tert-butyl alcohol; 2: Huisgen 1,3-dipolar cycloaddition reaction;
DOI:10.1021/jm300125e

Reference yield:

: 1484-12-4
N-methylcarbazole

: 1372602-87-3
3-(1-(4-(4-tert-butylphenyl)-1H-1,2,3-triazol-1-yl)ethyl)-9-methyl-9H-carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / chloroform / 0.75 h / 20 °C

2: sodium tetrahydroborate / methanol; dichloromethane / 1 h / 0 - 20 °C

3: indium(III) chloride; trimethylsilylazide / nitromethane / 0.5 h / 60 °C

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate; 4-nitro-benzoic acid / water; tert-butyl alcohol / 1 h / 20 °C

With indium(III) chloride; aluminum (III) chloride; sodium tetrahydroborate; copper(ll) sulfate pentahydrate; trimethylsilylazide; sodium L-ascorbate; 4-nitro-benzoic acid; In methanol; nitromethane; dichloromethane; chloroform; water; tert-butyl alcohol; 4: Huisgen 1,3-dipolar cycloaddition reaction;
DOI:10.1021/jm300125e