N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

Base Information

Chemical Name:N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide
CAS No.:320577-23-9
Molecular Formula:C₁₉H₃₀N₄O₄
Molecular Weight:378.472
Hs Code.:

Synonyms:N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

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Chemical Property of N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

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Technology Process of N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

There total 1 articles about N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 31972-52-8
Boc-Gly-Gly-OH

: 14165-18-5
N-benzyl-N-methylethylenediamine

: 320577-23-9
N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jm0010062

Reference yield: 81.0%

: 320577-23-9
N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

: 320577-28-4
N-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 24h;
DOI:10.1021/jm0010062

Reference yield:

: 320577-23-9
N-tert-butyloxycarbonyl-glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

: N-(1-piperidinomethylcarbonyl)glycyl-glycine-2-[(methylphenylmethyl)amino]ethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / HCl (gas) / ethyl acetate / 24 h / 20 °C

2: 80 percent / HOBT; DCC / CH₂Cl₂ / 60 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;
DOI:10.1021/jm0010062