C₄₁H₄₆N₂O₈S

Base Information

Chemical Name:C₄₁H₄₆N₂O₈S
CAS No.:1421947-65-0
Molecular Formula:C₄₁H₄₆N₂O₈S
Molecular Weight:726.891
Hs Code.:

C<sub>41</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₄₁H₄₆N₂O₈S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₆N₂O₈S

Chemical Property:

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Technology Process of C₄₁H₄₆N₂O₈S

There total 11 articles about C₄₁H₄₆N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421947-63-8
C₉H₈IN₃

: 1421947-65-0
C₄₁H₄₆N₂O₈S

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; water / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 3: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tet.2012.12.064

Reference yield:

: 1421947-64-9
C₉H₁₀IN

: 1421947-65-0
C₄₁H₄₆N₂O₈S

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; dichloromethane; 2: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tet.2012.12.064

Reference yield:

: 1608-48-6
3-Methyl-1,2-diiodobenzene

: 1421947-65-0
C₄₁H₄₆N₂O₈S

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Inert atmosphere; Reflux

2: potassium carbonate / acetone / 0.5 h / Inert atmosphere; Reflux

3: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 0.5 h / 20 °C / Inert atmosphere

4: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 16 h / 20 °C / Inert atmosphere

5: methanol; potassium fluoride / methanol / 1 h / 20 °C / Inert atmosphere

6: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

With methanol; potassium fluoride; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; acetone; 3: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling / 6: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tet.2012.12.064