ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate

Base Information

• Chemical Name: ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate
• CAS No.: 1058227-17-0
• Molecular Formula: C₁₉H₃₄NO₅PS
• Molecular Weight: 419.522

Synonyms:ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate

Chemical Property of ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate

Chemical Property:

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Technology Process of ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate

There total 1 articles about ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide (874291-45-9) + ethyl diethoxymethylphosphinate (65600-74-0) → ethyl diethoxymethyl-(SS,RC,RP)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate (1058227-17-0) + ethyl diethoxymethyl-(SS,RC,SP)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate (1058227-35-2)

Guidance literature:

With rubidium carbonate; In dichloromethane; at 20 ℃; optical yield given as %de; Inert atmosphere;

DOI:10.1002/chem.200800690

Reference yield: 94.0%

ethyl diethoxymethyl-(SS,RC,RP)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate (1058227-17-0) → (R)-1-amino-1-phenylethylphosphinic acid (1058227-57-8)

Guidance literature:

ethyl diethoxymethyl-(S_S,R_C,R_P)-(+)-(1-(tert-butylsulfinylamino)-(1-phenylethyl))phosphinate; With hydrogenchloride; In water; for 10h; Inert atmosphere; Reflux;

With methyloxirane; In ethanol; for 24h; optical yield given as %ee;

DOI:10.1002/chem.200800690

upstream raw materials:

(S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide

ethyl diethoxymethylphosphinate

Downstream raw materials:

(R)-1-amino-1-phenylethylphosphinic acid

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