(C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆

Base Information

• Chemical Name: (C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆
• CAS No.: 1356176-13-0
• Molecular Formula: C₃₂H₃₂N₂Rh*F₆Sb
• Molecular Weight: 783.265

Synonyms:(C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆

Chemical Property of (C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆

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Technology Process of (C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆

There total 6 articles about (C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄)(NC₅H₄C₆H₅))SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-phenylpyridine (1008-89-5) + silver hexafluoroantimonate (26042-64-8) + rac-(T-4)-chloro(η5-pentamethylcyclopentadienyl)(2-phenylene-κC(1'),pyridine-κN)rhodium(III) (945491-50-9) → (C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5)(1+)*SbF6(1-)=((C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5))SbF6 (1356176-13-0)

Guidance literature:

In dichloromethane; ligand, Rh complex and AgSbF6 in CH2Cl2 reacted at room temp. for 24 h;

DOI:10.1021/ja211110h

Reference yield:

2-phenylpyridine (1008-89-5) + C36H38N2O2RhS(1+)*F6Sb(1-) → (C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5)(1+)*SbF6(1-)=((C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5))SbF6 (1356176-13-0) + C26H24N2O2S

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1002/anie.201209887

Reference yield:

2-phenylpyridine (1008-89-5) + (C5(CH3)5)Rh(NC5H4C6H4CH(C6H5)NC(O)OCH(CH3)2)(1+)*SbF6(1-)=((C5(CH3)5)Rh(NC5H4C6H4CH(C6H5)NCOOCH(CH3)2))SbF6 (1356176-10-7) → (C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5)(1+)*SbF6(1-)=((C5(CH3)5)Rh(NC5H4C6H4)(NC5H4C6H5))SbF6 (1356176-13-0)

Guidance literature:

In dichloromethane; byproducts: NC5H4C6H4CH(Ph)NHCOO-i-Pr; Rh complex treated with ligand (2 equiv.) in CH2Cl2 at room temp. for 1.5 h;

DOI:10.1021/ja211110h

upstream raw materials:

2-phenylpyridine

silver hexafluoroantimonate

rac-(T-4)-chloro(η5-pentamethylcyclopentadienyl)(2-phenylene-κC(1'),pyridine-κN)rhodium(III)

(C₅(CH₃)5)Rh(NC₅H₄C₆H₄CH(C₆H₅)NC(O)OCH(CH₃)2)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄CH(C₆H₅)NCOOCH(CH₃)2))SbF₆

Downstream raw materials:

NC₅H₄C₆H₄CH(C₆H₅)NHC(O)OCH(CH₃)2

(C₅(CH₃)5)Rh(NC₅H₄C₆H₄CH(C₆H₅)NC(O)OCH(CH₃)2)⁽¹⁺⁾*SbF₆^(1-)=((C₅(CH₃)5)Rh(NC₅H₄C₆H₄CH(C₆H₅)NCOOCH(CH₃)2))SbF₆

N-[2-(pyridine-2-yl)phenyl]benzamide

N-phenyl-2-(pyridin-2-yl)benzamide

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