4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

Base Information

Chemical Name:4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester
CAS No.:132047-12-2
Molecular Formula:C₃₈H₆₀F₉O₅P
Molecular Weight:798.851
Hs Code.:

Synonyms:4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

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Chemical Property of 4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

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Technology Process of 4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

There total 6 articles about 4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phenyl-acetic acid 1-trifluoromethyl-nonyl ester

: 132047-12-2
4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (-) hapten 8, aq. Na₂HPO₄, aq. KH₂PO₄ / 15 h / 25 - 27 °C / pH 7.3

2: 45 percent / 5 h / 40 - 41 °C / cellulase, pH 7.3

3: pyridine / CH₂Cl₂

With pyridine; disodium hydrogenphosphate; potassium dihydrogenphosphate; (-) hapten 8; In dichloromethane;
DOI:10.1021/ja00006a032

Reference yield:

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 132047-12-2
4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / 5 h / 200 °C

2: conc. HCl / 1 h / Heating

3: thionyl chloride

4: pyridine / CH₂Cl₂

With pyridine; hydrogenchloride; thionyl chloride; In dichloromethane;
DOI:10.1021/ja00006a032

Reference yield:

: 14295-52-4
4-(diethyoxyphosphorylmethyl)benzoic acid methyl ester

: 132047-12-2
4-[Bis-((R)-1-trifluoromethyl-nonyloxy)-phosphorylmethyl]-benzoic acid (R)-1-trifluoromethyl-nonyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / 1 h / Heating

2: thionyl chloride

3: pyridine / CH₂Cl₂

With pyridine; hydrogenchloride; thionyl chloride; In dichloromethane;
DOI:10.1021/ja00006a032