N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

Base Information

Chemical Name:N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate
CAS No.:1421333-92-7
Molecular Formula:C₂HF₃O₂*C₁₂H₁₃Cl₂NO
Molecular Weight:372.171
Hs Code.:

Synonyms:N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

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Technology Process of N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

There total 5 articles about N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421333-91-6
tert-butyl 3-(2,4-dichlorophenoxy)propyl(prop-2-ynyl)carbamate

: 76-05-1
trifluoroacetic acid

: 1421333-92-7
N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

Reference yield:

: 1421333-90-5
tert-butyl 3-(2,4-dichlorophenoxy)propylcarbamate

: 1421333-92-7
N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; toluene / 20 °C / Inert atmosphere; Cooling with ice

2: N,N-dimethyl-formamide / 0.5 h / 20 °C

With sodium hydride; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 1421333-92-7
N-(3-(2,4-dichlorophenoxy)propy)prop-2-yn-1-aminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water / 3 h / Reflux

2: sodium azide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: hydrogen; palladium on activated charcoal / tert-butyl methyl ether / 21 h / 20 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; toluene / 20 °C / Inert atmosphere; Cooling with ice

5: N,N-dimethyl-formamide / 0.5 h / 20 °C

With sodium azide; palladium on activated charcoal; hydrogen; sodium hydride; sodium hydroxide; In tert-butyl methyl ether; water; N,N-dimethyl-formamide; toluene;