2-azido propionamido-N-3-phenylglyoxyl

Base Information

Chemical Name:2-azido propionamido-N-3-phenylglyoxyl
CAS No.:1401404-10-1
Molecular Formula:C₁₁H₁₀N₄O₃
Molecular Weight:246.225
Hs Code.:

Synonyms:2-azido propionamido-N-3-phenylglyoxyl

Suppliers and Price of 2-azido propionamido-N-3-phenylglyoxyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-azido propionamido-N-3-phenylglyoxyl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-azido propionamido-N-3-phenylglyoxyl

There total 3 articles about 2-azido propionamido-N-3-phenylglyoxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1401341-45-4
N-(3-acetylphenyl)-2-azidopropionamide

: 1401404-10-1
2-azido propionamido-N-3-phenylglyoxyl

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/ja308871v

Reference yield:

: 99-03-6
1-(3-aminophenyl)ethanone

: 1401404-10-1
2-azido propionamido-N-3-phenylglyoxyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / N,N-dimethyl-formamide / 0 °C

1.2: 3 h / 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

3.1: selenium(IV) oxide / 1,4-dioxane; water / 24 h / Inert atmosphere; Reflux

With selenium(IV) oxide; sodium azide; triethylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja308871v

Reference yield:

: 1017663-87-4
N-(3-acetylphenyl)-2-bromopropionamide

: 1401404-10-1
2-azido propionamido-N-3-phenylglyoxyl

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2: selenium(IV) oxide / 1,4-dioxane; water / 24 h / Inert atmosphere; Reflux

With selenium(IV) oxide; sodium azide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja308871v