2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

Base Information

Chemical Name:2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one
CAS No.:1309689-59-5
Molecular Formula:C₂₂H₂₄N₂O₂S
Molecular Weight:380.511
Hs Code.:

Synonyms:2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

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Chemical Property of 2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

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Technology Process of 2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

There total 3 articles about 2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5554-54-1
1,2,2,6,6-pentamethyl-4-piperidone

: 1309689-59-5
2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-trimethylammonium hydroxide; ammonium chloride / methanol; dimethyl sulfoxide / 5 h / 20 - 50 °C

2: tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 3 h / 150 °C / Inert atmosphere

With tri-tert-butyl phosphine; palladium diacetate; N-benzyl-trimethylammonium hydroxide; ammonium chloride; caesium carbonate; copper(I) bromide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05764a

Reference yield:

: 2942-13-4
6-methoxy-1,3-benzothiazole

: 1309689-58-4
2-(4-bromophenyl)-2,6,6-trimethylpiperidin-4-one

: 1309689-59-5
2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

Guidance literature:: With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; copper(I) bromide; In N,N-dimethyl-formamide; at 150 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c0cc05764a

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1309689-59-5
2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-trimethylammonium hydroxide; ammonium chloride / methanol; dimethyl sulfoxide / 5 h / 20 - 50 °C

2: tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 3 h / 150 °C / Inert atmosphere

With tri-tert-butyl phosphine; palladium diacetate; N-benzyl-trimethylammonium hydroxide; ammonium chloride; caesium carbonate; copper(I) bromide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05764a