(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

Base Information

Chemical Name:(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane
CAS No.:753017-95-7
Molecular Formula:C₂₆H₄₃NO₃
Molecular Weight:417.632
Hs Code.:

Synonyms:(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

Chemical Property:

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Technology Process of (4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

There total 5 articles about (4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 753017-93-5
(4S,5R,1'E)-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-5-trifluoroacetylamino-[1,3]dioxane

: 753017-95-7
(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

Guidance literature:: With sodium hydroxide; In ethanol; at 80 ℃;
DOI:10.1021/ja047597t

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 753017-95-7
(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

Guidance literature:: Multi-step reaction with 5 steps

1: TsOH / dimethylformamide / 20 °C

2: TBAF / tetrahydrofuran / 20 °C

3: pyridine / 0 °C

4: 57 percent / Li₂CuCl₄ / tetrahydrofuran / -15 °C

5: aq. NaOH / ethanol / 80 °C

With pyridine; sodium hydroxide; dilithium tetrachlorocuprate; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja047597t

Reference yield:

: 753017-92-4
(4S,5R,1'E)-4-(3'-acetoxypent-1'-enyl)-2-(4''-methoxyphenyl)-5-trifluoroacetylamino-[1,3]dioxane

: 753017-95-7
(4S,5R,1'E)-5-amino-2-(4''-methoxyphenyl)-4-(pentadec-1'-enyl)-[1,3]dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / Li₂CuCl₄ / tetrahydrofuran / -15 °C

2: aq. NaOH / ethanol / 80 °C

With sodium hydroxide; dilithium tetrachlorocuprate; In tetrahydrofuran; ethanol;
DOI:10.1021/ja047597t