phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

Base Information

Chemical Name:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside
CAS No.:1030632-33-7
Molecular Formula:C₂₅H₄₀O₅Si
Molecular Weight:448.675
Hs Code.:

Synonyms:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

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Technology Process of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

There total 1 articles about phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1030632-29-1
phenylmethyl 4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1030632-33-7
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

Guidance literature:: With 1H-imidazole; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ol800697k

Reference yield: 95.0%

: 1030632-33-7
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[(2S,6R)-3,6-dihydro-6-methyl-2H-pyran-2-yl]-β-D-olivopyranoside

: 1030632-35-9
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[2,6-dideoxy-β-D-ribo-hexopyranosyl]-β-D-olivopyranoside

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In dichloromethane; at 0 ℃; diastereoselective reaction;
DOI:10.1021/ol800697k