N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

Base Information

Chemical Name:N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide
CAS No.:1374511-02-0
Molecular Formula:C₂₃H₂₀N₄O₃S
Molecular Weight:432.503
Hs Code.:

Synonyms:N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

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Chemical Property of N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

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Technology Process of N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

There total 5 articles about N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374511-01-9
C₁₆H₁₆N₄OS

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1374511-02-0
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

: 1374511-26-8
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

Guidance literature:: With acetic acid; In ethanol; at 90 ℃; for 2h; optical yield given as %de;
DOI:10.1016/j.bmcl.2012.03.061

Reference yield:

: 4857-04-9
2-chloromethyl-1H-benzimidazole

: 1374511-02-0
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

: 1374511-26-8
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / 2 h / Reflux

1.2: 0.5 h / 20 °C

2.1: potassium carbonate / acetone / 6 h / 20 °C

3.1: hydrazine hydrate / ethanol / 7 h / 20 °C

4.1: acetic acid / ethanol / 2 h / 90 °C

With potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; acetone;
DOI:10.1016/j.bmcl.2012.03.061

Reference yield:

: 1374511-00-8
tert-butyl 2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetate

: 1374511-02-0
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

: 1374511-26-8
N'-(2,4-dihydroxybenzylidene)-2-(2-(phenylthiomethyl)-1H-benzo[d]imidazol-1-yl)acetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 7 h / 20 °C

2: acetic acid / ethanol / 2 h / 90 °C

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.bmcl.2012.03.061