7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

Base Information

Chemical Name:7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one
CAS No.:871669-32-8
Molecular Formula:C₁₇H₁₈O₅
Molecular Weight:302.327
Hs Code.:

Synonyms:7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

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Chemical Property of 7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

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Technology Process of 7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

There total 6 articles about 7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871669-30-6
7α-trimethylsilyloxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

: 871669-32-8
7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

Guidance literature:: With hydrogenchloride; In acetone; at 20 ℃; for 0.166667h; Yield given;

Reference yield:

: 32233-40-2
(3aR,4S,5R,6aS)-5-hydroxy-4-(hydroxymethyl)hexahydro-2H-cyclopenta[b]furan-2-one

: 871669-32-8
7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 1 h / 145 °C

2: CrO₃/pyridine, activated silica gel / CH₂Cl₂ / 0.42 h

3: KOH / CH₂Cl₂ / 0.33 h / Ambient temperature

4: 1 N hydrochloric acid / acetone / 0.17 h / 20 °C

With pyridine; chromium(VI) oxide; hydrogenchloride; potassium hydroxide; silica gel; In dichloromethane; acetone;

Reference yield:

: 40665-68-7
dimethyl (3-phenoxy-2-oxopropyl)phosphonate

: 871669-32-8
7α-hydroxy-6β-(3'-oxo-4'-phenoxy-1'E-butenyl)-2-oxabicyclo<3.3.0>octan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 1 N hydrochloric acid / acetone / 0.17 h / 20 °C

With hydrogenchloride; potassium hydroxide; In dichloromethane; acetone;