4-(4-FLUOROPHENYL)AMINOCARBONYLPHENYLBORONIC ACID

Base Information

• Chemical Name: 4-(4-FLUOROPHENYL)AMINOCARBONYLPHENYLBORONIC ACID
• CAS No.: 850568-27-3
• Molecular Formula: C13H11 B F N O3
• Molecular Weight: 259.045
• Hs Code.: 2931900090
• Mol file: 850568-27-3.mol

Synonyms:Boronicacid, [4-[[(4-fluorophenyl)amino]carbonyl]phenyl]- (9CI);[4-[(4-Fluorophenyl)carbamoyl]phenyl]boronic acid

Chemical Property of 4-(4-FLUOROPHENYL)AMINOCARBONYLPHENYLBORONIC ACID

Chemical Property:

• Melting Point: 234-240
• Refractive Index: 1.606
• PSA: 69.56000
• Density: 1.34g/cm³
• LogP: 0.83080
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(4-Fluorophenyl)aminocarbonylphenylboronicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(4-FLUOROPHENYL)AMINOCARBONYLPHENYLBORONIC ACID

There total 1 articles about 4-(4-FLUOROPHENYL)AMINOCARBONYLPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-carboxyphenylboronic acid (14047-29-1) + 4-fluoroaniline (371-40-4) → C13H11BFNO3 (850568-27-3)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In dichloromethane;

DOI:10.1016/j.bmcl.2006.07.010

Reference yield:

C13H11BFNO3 (850568-27-3) + 4-methoxybenzyl (2S,3R)-3-((2-(bis(tert-butoxycarbonyl)amino)pyridin-4-yl)methyl)-4-oxoazetidine-2-carboxylate (911851-49-5) → C33H35FN4O8

Guidance literature:

With triethylamine; copper diacetate; In dichloromethane; at 20 ℃; Molecular sieve;

Reference yield:

C13H11BFNO3 (850568-27-3) + 2 chloro-3-methylpyridine (18368-76-8) → N-(4-fluoro-phenyl)-4-(3-methyl-pyridin-2-yl)-benzamide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; at 80 ℃;

DOI:10.1016/j.bmcl.2006.07.010

upstream raw materials:

4-carboxyphenylboronic acid

4-fluoroaniline

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