2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

Base Information

Chemical Name:2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate
CAS No.:679417-86-8
Molecular Formula:C₃₃H₄₁O₉P
Molecular Weight:612.657
Hs Code.:

Synonyms:2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

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Chemical Property of 2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

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Technology Process of 2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

There total 3 articles about 2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59591-01-4
2,2-diphenylcyclopropanecarbaldehyde

: 679417-86-8
2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 °C

2.1: tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane;
DOI:10.1021/jo0357972

Reference yield:

: 343986-63-0
2,4-dimethoxybenzyl 2-methoxypropionate

: 679417-86-8
2,4-dimethoxybenzyl 3-(diethylphosphatoxy)-3-(2,2-diphenylcyclopropyl)-2-methoxy-2-methylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 °C

2.1: tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane;
DOI:10.1021/jo0357972