11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Base Information

Chemical Name:11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate
CAS No.:1431987-02-8
Molecular Formula:C₂₀H₃₁NO₇
Molecular Weight:397.469
Hs Code.:

Synonyms:11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Suppliers and Price of 11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

There total 6 articles about 11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: di-tert-butyl 2,3-dimethoxy-5-methyl-6-(10-(nitrooxy)undecyl)-1,4-phenylene dicarbonate

: 1431987-02-8
11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Guidance literature:: di-tert-butyl 2,3-dimethoxy-5-methyl-6-(10-(nitrooxy)undecyl)-1,4-phenylene dicarbonate; With hydrogenchloride; In 1,4-dioxane; ethyl acetate; at 20 ℃;

With silver(l) oxide; In diethyl ether; for 2h;

Reference yield:

: 1431987-51-7
di-tert-butyl 2,3-dimethoxy-5-methyl-6-(10-oxodecyl)-1,4-phenylene dicarbonate

: 1431987-02-8
11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; diethyl ether / 1 h / -78 °C

2.1: 2,6-di-tert-butyl-4-methylpyridine; tetrabutylammonium nitrate; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 °C

3.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 20 °C

3.2: 2 h

With hydrogenchloride; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; ethyl acetate;

Reference yield:

: 1431987-52-8
di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

: 1431987-02-8
11-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)undecan-2-yl nitrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-di-tert-butyl-4-methylpyridine; tetrabutylammonium nitrate; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 °C

2.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 20 °C

2.2: 2 h

With hydrogenchloride; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; In 1,4-dioxane; dichloromethane; ethyl acetate;