di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Base Information

Chemical Name:di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate
CAS No.:1431987-52-8
Molecular Formula:C₃₀H₅₀O₉
Molecular Weight:554.722
Hs Code.:

Synonyms:di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Chemical Property:

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Technology Process of di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

There total 6 articles about di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 917-64-6
methyl magnesium iodide

: 1431987-51-7
di-tert-butyl 2,3-dimethoxy-5-methyl-6-(10-oxodecyl)-1,4-phenylene dicarbonate

: 1431987-52-8
di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h;

Reference yield:

: 1431987-50-6
di-tert-butyl 2-(10-hydroxydecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

: 1431987-52-8
di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 6 h / 0 °C

2: tetrahydrofuran; diethyl ether / 1 h / -78 °C

With pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 34619-03-9
tert-butyldicarbonate

: 1431987-52-8
di-tert-butyl 2-(10-hydroxyundecyl)-5,6-dimethoxy-3-methyl-1,4-phenylene dicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 0 - 20 °C

2: pyridinium chlorochromate / dichloromethane / 6 h / 0 °C

3: tetrahydrofuran; diethyl ether / 1 h / -78 °C

With triethylamine; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;