C₂₂H₂₂F₃NO₃S

Base Information

Chemical Name:C₂₂H₂₂F₃NO₃S
CAS No.:1415578-03-8
Molecular Formula:C₂₂H₂₂F₃NO₃S
Molecular Weight:437.483
Hs Code.:

C<sub>22</sub>H<sub>22</sub>F<sub>3</sub>NO<sub>3</sub>S

Synonyms:C₂₂H₂₂F₃NO₃S

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Chemical Property of C₂₂H₂₂F₃NO₃S

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Technology Process of C₂₂H₂₂F₃NO₃S

There total 8 articles about C₂₂H₂₂F₃NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415578-02-7
C₂₉H₂₈F₃NO₃S

: 1415578-03-8
C₂₂H₂₂F₃NO₃S

Guidance literature:: With hydrogen bromide; acetic acid; at 100 ℃; for 0.5h;

Reference yield:

: 76041-72-0
2-mercapto-5-trifluoromethylpyridine

: 1415578-03-8
C₂₂H₂₂F₃NO₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / tetrahydrofuran / 1.5 h / 0 °C / Cooling with ice

2.1: chloroform / 8 h / 0 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

3.2: 0.5 h / Reflux

4.1: water; sodium carbonate / 5 h / Reflux

5.1: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere

6.1: acetic acid; hydrogen bromide / 0.5 h / 100 °C

With dmap; water; hydrogen bromide; sodium methylate; sodium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; chloroform; toluene; 2.1: |Wittig Olefination;

Reference yield:

: 114449-80-8
C₉H₈F₃NOS

: 1415578-03-8
C₂₂H₂₂F₃NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: chloroform / 8 h / 0 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

2.2: 0.5 h / Reflux

3.1: water; sodium carbonate / 5 h / Reflux

4.1: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere

5.1: acetic acid; hydrogen bromide / 0.5 h / 100 °C

With dmap; water; hydrogen bromide; sodium methylate; sodium carbonate; acetic acid; In tetrahydrofuran; methanol; chloroform; toluene; 1.1: |Wittig Olefination;