Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

Base Information

Chemical Name:Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester
CAS No.:1026632-80-3
Molecular Formula:C₃₂H₄₇NO₄
Molecular Weight:509.729
Hs Code.:

Synonyms:Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

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Chemical Property of Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

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Technology Process of Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

There total 7 articles about Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1026632-80-3
Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 30 g / NaOH / (C₈H₁₇)3NCH₃⁺Cl^- / toluene; H₂O / 65 h / Heating

2: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

3: pyridine / tetrahydrofuran

4: 91 percent / dimethylformamide / 2 h / Heating

5: 77 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

6: pyridine / CH₂Cl₂

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; (C₈H₁₇)3NCH₃⁺Cl^-; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00104a002

Reference yield:

: 112-71-0
1-Bromotetradecane

: 1026632-80-3
Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 30 g / NaOH / (C₈H₁₇)3NCH₃⁺Cl^- / toluene; H₂O / 65 h / Heating

2: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

3: pyridine / tetrahydrofuran

4: 91 percent / dimethylformamide / 2 h / Heating

5: 77 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

6: pyridine / CH₂Cl₂

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; (C₈H₁₇)3NCH₃⁺Cl^-; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00104a002

Reference yield:

: 94741-95-4
1-nitro-4-(tetradecyloxy)benzene

: 1026632-80-3
Acetic acid 3-{[acetyl-(4-tetradecyloxy-phenyl)-amino]-methyl}-benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

2: pyridine / tetrahydrofuran

3: 91 percent / dimethylformamide / 2 h / Heating

4: 77 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

5: pyridine / CH₂Cl₂

With pyridine; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00104a002