phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

Base Information

Chemical Name:phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate
CAS No.:1375744-85-6
Molecular Formula:C₁₉H₂₂N₂O₄
Molecular Weight:342.395
Hs Code.:

Synonyms:phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

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Chemical Property of phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

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Technology Process of phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

There total 1 articles about phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 68579-60-2,6589-55-5
2-(methylamino)-1-phenylethanol

: 1096711-35-1
phenyl (2-chloro-2-oxoethyl)methylcarbamate

: 1375744-85-6
phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; at 0 ℃;
DOI:10.1021/jo3007144

Reference yield: 93.0%

: 1375744-85-6
phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

: 1375744-65-2
phenyl N-methyl-N-{[methyl(2-oxo-2-phenylethyl)carbamoyl]methyl}carbamate

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 0 ℃; Molecular sieve;
DOI:10.1021/jo3007144

Reference yield:

: 1375744-85-6
phenyl N-{[(2-hydroxy-2-phenylethyl)(methyl)carbamoyl]methyl}-N-methylcarbamate

: 1215725-23-7
3-benzoyl-1,4-dimethylpiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; pyridinium chlorochromate / dichloromethane / 0 °C / Molecular sieve

2: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 70 °C

With sodium acetate; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; mineral oil; 2: Dieckmann cyclization;
DOI:10.1021/jo3007144